Figure 3.
Deconvoluted C1s XPS spectra (a), XPS general spectra (b), the atomic ratio of O/C (violet) and the relative amounts of sp2 C=C, C-H, sp3 C-C, C-O/C-O-C, C=O and O=C-O bonds calculated based on the deconvoluted C1s XPS spectra (colours) illustrating the evolution of each group for GO and GNM-2, 3, 4, 5h (c), the relative amounts of non-oxygen functional groups (d) and oxygen functional groups (4) as a function of reaction time.