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Robustness of method.
| Chromatographic Conditions | Variation | Retention time (Minutes) | |||
|---|---|---|---|---|---|
| PCM | MP | PP | CTZ | ||
| Temprature (ºC) | 23 | 3.42 | 4.64 | 6.63 | 7.609 |
| 27 | 3.57 | 4.69 | 6.8 | 7.701 | |
| Flow rate (mL min-1) | 0.8 | 3.75 | 4.56 | 6.48 | 7.31 |
| 1.2 | 3.28 | 4.97 | 6.96 | 7.93 | |
| Vol. of Acetonitrile (%) | 43 | 3.67 | 4.71 | 6.75 | 7.83 |
| 47 | 3.37 | 4.54 | 6.56 | 7.55 | |
