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. 2016 Aug 9;72(Pt 9):667–671. doi: 10.1107/S2053230X16011419

Table 3. Data collection and processing.

Diffraction source Beamline I04, DLS
Wavelength (Å) 0.9795
Temperature (K) 100
Detector Pilatus 6M-F
Rotation range per image (°) 0.10
Total rotation range (°) 180
Exposure time per image (s) 0.040
Space group P21
a, b, c (Å) 48.04, 78.31, 67.71
α, β, γ (°) 90, 99.94, 90
ISa 12.0
Resolution range (Å) 18.6–1.35 (1.39–1.35)
Total No. of reflections 357812 (26206)
No. of unique reflections 107545 (7947)
Completeness (%) 99.4 (99.6)
Multiplicity 3.3 (3.3)
I/σ(I)〉 7.1 (1.3)
R meas 0.098 (0.970)
Overall B factor from Wilson plot (Å2) 15.2

Mean I/σ(I) < 2.0 at 1.45 Å.