Table 1. Data collection and processing.
| D4/A201–50-W43A | D4-R167A/A201–50 | D4-P173G/A201–50 | |
|---|---|---|---|
| Resolution range (Å) | 48.51–2.59 (2.71–2.59) | 28.84–2.80 (2.95–2.80) | 48.61–2.49 (2.59–2.49) |
| No. of observed reflections | 297885 (34796) | 181073 (25880) | 248402 (26386) |
| No. of unique reflections | 23077 (2648) | 18696 (2618) | 26149 (2811) |
| Completeness (%) | 99.6 (95.5) | 99.6 (97.5) | 99.5 (96.0) |
| Multiplicity | 12.9 (13.6) | 9.7 (9.9) | 9.5 (9.4) |
| Mean I/σ(I) | 16.1 (3.2) | 15.4 (3.5) | 19.7 (3.8) |
| R r.i.m. † | 0.099 (0.779) | 0.113 (0.695) | 0.073 (0.573) |
| Mosaicity (°) | 0.21 | 0.22 | 0.26 |
| Overall B factor from Wilson plot (Å2) | 56.8 | 52.1 | 47.4 |
†
Estimated R r.i.m. = R merge × [N/(N − 1)]1/2, where N is the data multiplicity.