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. 2016 Aug 31;72(Pt 9):1036–1048. doi: 10.1107/S2059798316012304

Table 2. Data-collection and processing statistics for the fast rotation experiment.

Values in parentheses are for the outer shell.

Data set lys_3 lys_4 lys_5 lys_6 lys_7 lys_8 lys_9 lys_10
Wavelength (Å) 1.0332 1.0332 1.0332 1.0332 1.0332 1.0332 1.0332 1.0332
Temperature (K) 100 100 100 100 100 100 100 100
EIGER detector 1M 1M 1M 1M 1M 1M 1M 1M
Detector distance (mm) 50 50 50 50 50 50 50 50
Resolution (Å) 1.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5
Total rotation range (°) 180 180 180 180 180 180 180 180
Rotation range per image (°) 0.00125 0.0125 0.025 0.05625 0.1125 0.225 0.45 0.9
No. of images 144000 14400 7200 3200 1600 800 400 200
Exposure time (s) 0.00125 0.00125 0.00125 0.00125 0.00125 0.00125 0.00125 0.00125
Beam transmission 0.001 0.01 0.02 0.045 0.09 0.18 0.36 0.72
Rotation speed (° s−1) 1 10 20 45 90 180 360 720
Space group P43212 P43212 P43212 P43212 P43212 P43212 P43212 P43212
Unit-cell parameters
a = b (Å) 77.98 78.31 78.32 78.32 78.35 78.38 78.37 78.38
c (Å) 36.95 37.02 37.02 37.04 37.03 37.04 37.04 37.05
 α = β = γ (°) 90 90 90 90 90 90 90 90
Mosaicity (°) 0.23 0.22 0.22 0.22 0.23 0.23 0.24 0.27
No. of reflections 248970 251327 251572 251909 251489 251726 253181 252979
No. of unique reflections 18845 19011 18994 18987 18965 18998 18979 18994
Completeness (%) 99.5 (97.9) 99.2 (96.1) 99.2 (96.1) 99.3 (96.4) 99.5 (97.6) 99.6 (98.5) 99.5 (98.1) 99.5 (98.2)
Multiplicity 13.2 (10.0) 13.2 (9.9) 13.2 (10.0) 13.3 (10.0) 13.3 (10.1) 13.3 (10.0) 13.3 (10.1) 13.3 (10.0)
ISa 24.2 22.4 22.1 21.2 21.9 19.3 15.4 11.9
I/σ(I)〉 23.8 (3.5) 23.8 (3.4) 22.7 (3.4) 21.5 (2.8) 22.2 (2.5) 21.3 (2.4) 20.1 (2.6) 17.6 (2.5)
R meas (%) 6.9 (50.4) 6.8 (52.8) 7.2 (53.8) 7.5 (71.1) 7.4 (86.2) 7.7 (90.3) 8.6 (93.0) 10.2 (108.1)
CC1/2 (%) 100 (77.4) 99.9 (80.0) 99.9 (78.4) 99.9 (75.3) 99.9 (75.9) 99.9 (77.4) 99.9 (76.3) 99.8 (73.8)

Beam transmission is presented as a fraction of the full beam (3.6 × 1012 photon s−1).