Table 1. Crystallography statistics.
| Data Collection | |
|---|---|
| Space group | P21212 |
| Unit cell parameters (Å) | a = 45.21, b = 130.33, c = 136.71 |
| Resolution (Å) | 60.53–2.30 (2.38–2.30) |
| Rmerge | 10.9 (89.9) |
| Rpim | 6.5 (54.9) |
| Unique Reflections | 36905 (3585) |
| <I/σ(I)> | 14.0 (2.6) |
| Completeness (%) | 100.0 (99.9) |
| Multiplicity | 7.2 (7.0) |
| Anomalous completeness (%) | 98.9 (94.0) |
| Anomalous multiplicity | 3.7 (3.4) |
| Refinement | |
| Resolution (Å) | 47.2–2.3 |
| No. reflections | 69289 |
| No. reflections (non-anomalous) | 36828 |
| Rwork/Rfree | 18.1/23.7 |
| No. total atoms | 5912 |
| B factors | |
| Wilson (Å2) | 30.4 |
| Average (Å2) | |
| Chain A | 36.0 |
| Chain B | 39.3 |
| Chain C | 34.9 |
| Chain D | 35.8 |
| Waters | 33.4 |
| Rms deviations | |
| Bond lengths (Å) | 0.014 |
| Bond angles (°) | 1.159 |
| Molprobity statistics | |
| Ramachandran favored (%) | 96.38 |
| Allowed (%) | 3.62 |
| Outliers (%) | 0.00 |
| All-atom clashscore | 2.98 |
| Solvent content (%) | 44.1% |