Extended Data Table 3. Data collection and refinement statistics.
E2Ubc9-SUMO/E3sizl-SUMO/PCNA | |
---|---|
Data collection | |
Space group | C121 |
Cell dimensions | |
a, b, c (Å) | 93.42, 205.88, 142.50 |
α, β, γ (°) | 90.00, 95.30, 90.00 |
Resolution (Å) | 48.4-2.85 (2.95-2.85)* |
Rmerge | 10.7 (55.6) |
I/σI | 9.1 (1.82) |
Completeness (%) | 99.0 (98.0) |
Redundancy | 3.6 (2.9) |
Refinement | |
Resolution (Å) | 47.3-2.85 |
No. reflections | 61981 |
Rwork / Rfree | 0.210/0.248 |
No. atoms | 13744 |
Protein | 13403 |
Ligand/ion | 70 |
Water | 271 |
B-factors | |
Protein | 58.3 |
Ligand/ion | 64.5 |
Water | 43.0 |
R.m.s. deviations | |
Bond lengths (Å) | 0.001 |
Bond angles (°) | 0.42 |
Values in parentheses are for highest-resolution shell.