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. 2016 Aug 31;113(37):10358–10363. doi: 10.1073/pnas.1605442113

Table S1.

Data collection and refinement statistics for AdiC

Data collection and refinement AgmAdiC-wt apoAdiC-wt
Data collection
 Wavelength (Å) 1.0 1.0
 Space group P 21 21 2 P 21 21 2
 Unit-cell parameters,
  a, b, c (Å); α =β = γ (°) 104.8, 175.6, 72.9; 90 104.8, 175.4, 73.2; 90
 Resolution (Å) 49.44–2.59 (2.73–2.59) 49.51–2.21 (2.33–2.21)
 No. of observed reflections 280,724 (38,770) 401,210 (52,895)
 No. of unique reflections 41,837 (5,764) 68,197 (9,571)
Rmerge (%) 10.9 (117) 7.1 (114)
 Completeness (%) 98.7 (94.9) 99.4 (96.8)
 Multiplicity 6.7 (6.7) 5.9 (5.5)
II 12.0 (1.6) 14.9 (1.5)
 CC1/2 (%) 99.9 (71.3) 99.9 (58.9)
Refinement
 Resolution (Å) 49.45–2.59 49.52–2.21
Rwork/Rfree (%) 22.09/25.07 19.72/21.01
 No. of atoms
  Protein 6,484 6,480
  Ligand 18
  Water 12 159
 Mean B factor (Å2) 68.8 60.1
  Protein 68.7 60.2
  Ligand 70.5
  Water 57.3 55.8
 Rmsd
  Bond length (Å) 0.007 0.007
  Bond angle (°) 0.922 0.996
 Ramachandran plot (%)
  Favored region 99.1 99.7
  Allowed region 100 100
  Disallowed region 0 0

Values in parentheses reflect the highest-resolution shell.