Skip to main content
. Author manuscript; available in PMC: 2017 May 25.
Published in final edited form as: J Am Chem Soc. 2016 May 11;138(20):6372–6375. doi: 10.1021/jacs.6b02653

Table 2.

Tandem Ring-Opening Cross Metathesis/Oxidative Cyclization of 1,5-Cyclooctadiene with Terminal Olefins

graphic file with name nihms-813235-f0005.jpg
Entry Terminal olefin Product Isolated Yield (%)a
1 graphic file with name nihms-813235-t0006.jpg graphic file with name nihms-813235-t0007.jpg 50
2 graphic file with name nihms-813235-t0008.jpg graphic file with name nihms-813235-t0009.jpg 57% (52%)b
3 graphic file with name nihms-813235-t0010.jpg graphic file with name nihms-813235-t0011.jpg 41%c
a

Isolated as a single diastereomer.

b

Using 2.5 mmol of 3 (964 mg 2b isolated).

c

Isolated yield after benzoylation (for ease of purification).