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. 2016 Sep 23;6:33908. doi: 10.1038/srep33908

Table 2. 13C NMR spectroscopic data for compounds 1–8a.

No. 1 2 3 4 5 6 7 8
1 136.6 qC 109.2 qC 87.8 qC 214.5 qC 198.7 qC 199.3 qC 198.6 qC 32.6 CH2
2 36.2 CH 55.0 CH 46.3 CH 48.6 CH 130.4 qC 129.2 qC 128.4 qC 25.0 CH2
3 73.7 CH 76.3 CH 75.8 CH 77.1 CH 160.9 CH 158.3 CH 161.9 CH 75.9 CH
4 37.1 qC 39.4 qC 45.2 qC 39.4 qC 36.6 qC 36.8 qC 36.8 qC 36.9 qC
5 40.4 CH 41.7 CH 42.5 CH 42.4 CH 45.2 CH 43.0 CH 45.2 CH 41.8 CH
6 32.7 CH2 33.6 CH2 71.6 CH 33.3 CH2 34.8 CH2 34.7 CH2 34.6 CH2 23.2 CH2
7 174.5 qC 174.0 qC 170.0 qC 174.1 qC 173.5 qC 173.6 qC 173.4 qC 75.3 CH
8 75.5 qC 89.6 qC 73.3 qC 62.7 qC 201.0 qC 197.8 qC 80.1 qC 42.2 qC
9 98.2 qC 99.8 qC 31.0 CH 54.4 CH 79.8 qC 172.8 qC 208.2/208.0 qC 43.0 CH
10 119.7 qC 36.5 CH 47.2 qC 48.2 qC 43.2 CH 45.6 CH 42.8 CH 37.4 qC
11 28.2 CH2 33.0 CH2 28.8 CH2 18.5 CH2 29.5 CH2 29.4 CH2 32.9 CH2 16.2 CH2
12 25.5 CH2 27.1 CH2 71.0 CH 33.1 CH2 28.6 CH2 29.8 CH2 25.6 CH2 33.8 CH2
13 38.3 qC 36.1 qC 39.3 qC 40.3 qC 41.5 qC 41.4 qC 38.6/38.5 qC 46.6 qC
14 163.7 qC 35.6 CH 46.4 CH 71.8 qC 156.6 qC 158.9 qC 162.5 qC 159.6 qC
15 117.7 CH 29.0 CH2 28.0 CH2 40.8 CH2 121.2 CH 124.4 CH 117.7 CH 118.0 CH
16 165.5 qC 171.2 qC 169.7 qC 169.5 qC 163.4 qC 163.4 qC 164.5/164.3 qC 34.8 CH2
17 81.1 CH 79.4 CH 76.8 CH 78.4 CH 81.4 CH 78.5 CH 78.2/77.9 CH 58.1 CH
18 18.8 CH3 24.4 CH3 18.8 CH3 20.1 CH3 18.6 CH3 20.4 CH3 18.4/18.3 CH3 19.3 CH3
19 12.8 CH3 10.8 CH3 22.6 CH3 16.4 CH3 12.2 CH3 11.7 CH3 11.6 CH3 15.4 CH3
20 119.7 qC 120.9 qC 120.7 qC 120.1 qC 119.2 qC 119.6 qC 132.9 qC 37.5 CH
21 141.2 CH 140.8 CH 140.4 CH 141.2 CH 141.4 CH 141.6 CH 169.1/168.8 qC 72.6 CH2
22 109.8 CH 109.9 CH 109.1 CH 110.4 CH 109.7 CH 109.8 CH 150.4/149.7 CH 34.1 CH2
23 142.9 CH 143.3 CH 143.9 CH 142.9 CH 143.3 CH 143.4 CH 97.4/96.7 CH 176.8 qC
28 24.8 CH3 24.4 CH3 15.6 CH3 23.0 CH3 20.6 CH3 20.1 CH3 27.8 CH3 21.9 CH3
29 20.1 CH3 20.9 CH3 41.0 CH2 20.7 CH3 28.0 CH3 28.2 CH3 20.6 CH3 28.0 CH3
30 68.9 CH 71.3 CH 69.7 CH 62.8 CH 66.8 CH 41.3 CH2 67.8 CH 27.5 CH3
7-OMe 52.0 CH3 51.9 CH3 53.0 CH3 52.4 CH3 52.0 CH3 52.0 CH3 52.0 CH3  
9-OMe           51.8 CH3    
7-OAc               21.3 CH3
                170.4 qC
1-OAc     21.0 CH3          
      168.4 qC          
3-OAc   21.2 CH3 21.1 CH3          
    169.8 qC 169.4 qC          
6-OAc     21.0 CH3          
      169.6 qC          
12-OAc     22.1 CH3          
      169.7 qC          
30-OAc 20.7 CH3 20.9 CH3 21.4 CH3       21.0 CH3  
  170.5 qC 170.2 qC 170.7 qC       169.9/169.8 qC  
1′ 167.3 qC     167.0 qC 165.7 qC      
2′ 128.7 qC     127.4 qC 127.8 qC      
3′ 137.2 CH     140.4 CH 138.9 CH      
4′ 14.5 CH3     14.8 CH3 14.6 CH3      
5′ 12.1 CH3     12.3 CH3 12.0 CH3      

aSpectra measured at 100 MHz in CDCl3.