Table 1.
Position | 1 | 2 | ||
---|---|---|---|---|
δH | δC | δH | δC | |
2 | - | 164.8 | - | 164.5 |
3 | 6.83 (s) | 103.5 | - | 132.3 |
4 | - | 182.4 | - | 182.4 |
5 | - | 161.6 | - | 153 |
6 | 6.43 | 100 | 6.90 (s) | 92 |
7 | - | 163.3 | - | 159 |
8 | 6.75 | 95.2 | 6.82 (s) | 103.1 |
9 | - | 157.3 | - | 152.5 |
10 | - | 105.8 | - | 105.5 |
1’ | 5.04 (d, J=7.8) | 121.4 | - | 121.5 |
2’,6’ | 7.93 (d, J=8.8) | 129 | 7.94 (d, J=8) | 128.9 |
3’,5’ | 6.94 (d, J=8.8) | 116.5 | 6.91 (d, J=8) | 116.4 |
4’ | - | 161.7 | - | 161.7 |
Glc: 1" | 5.04 (d, J=7.8) | 100.3 | 60.4 | |
2" | 3.28 | 73.5 | 56.8 | |
3" | 3.26 (m) | 76.7 | - | |
4" | 3.14 (m) | 70 | ||
5" | 3.58 (m) | 76 | ||
6" | 3.84(d),3.41 (m) | 66.5 | ||
Rha: 1’" | 4.54 (s) | 100.9 | ||
2’" | 3.64 (bs) | 70.7 | ||
3’" | 3.41 (m) | 71.2 | ||
4’" | 3.13 (m) | 72.5 | ||
5’" | 3.44 (m) | 68.7 | ||
6’" | 1.06 (d, J=6) | 18.2 | ||
3-OMe | - | - | 3.72 | 60.4 |
7-OMe | - | - | 3.91 | 56.8 |
5-OH | - | - | 12.9 | - |
4’-OH | - | - | 10.36 | - |