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. 2016 Aug;19(8):804–811.

Table 1.

1H-NMR and 13C-NMR data of compounds 1 and 2 (600 MHz, DMSO-d6)

Position 1 2
δH δC δH δC
2 - 164.8 - 164.5
3 6.83 (s) 103.5 - 132.3
4 - 182.4 - 182.4
5 - 161.6 - 153
6 6.43 100 6.90 (s) 92
7 - 163.3 - 159
8 6.75 95.2 6.82 (s) 103.1
9 - 157.3 - 152.5
10 - 105.8 - 105.5
1’ 5.04 (d, J=7.8) 121.4 - 121.5
2’,6’ 7.93 (d, J=8.8) 129 7.94 (d, J=8) 128.9
3’,5’ 6.94 (d, J=8.8) 116.5 6.91 (d, J=8) 116.4
4’ - 161.7 - 161.7
Glc: 1" 5.04 (d, J=7.8) 100.3 60.4
2" 3.28 73.5 56.8
3" 3.26 (m) 76.7 -
4" 3.14 (m) 70
5" 3.58 (m) 76
6" 3.84(d),3.41 (m) 66.5
Rha: 1’" 4.54 (s) 100.9
2’" 3.64 (bs) 70.7
3’" 3.41 (m) 71.2
4’" 3.13 (m) 72.5
5’" 3.44 (m) 68.7
6’" 1.06 (d, J=6) 18.2
3-OMe - - 3.72 60.4
7-OMe - - 3.91 56.8
5-OH - - 12.9 -
4’-OH - - 10.36 -