Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C32H34N4O2 |
| M r | 506.63 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 5.1776 (3), 27.9346 (17), 8.7893 (6) |
| β (°) | 96.203 (2) |
| V (Å3) | 1263.79 (14) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.08 |
| Crystal size (mm) | 0.20 × 0.15 × 0.12 |
| Data collection | |
| Diffractometer | Bruker SMART APEX CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2003 ▸) |
| T min, T max | 0.783, 0.990 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 15125, 2243, 1469 |
| R int | 0.073 |
| (sin θ/λ)max (Å−1) | 0.596 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.050, 0.127, 1.02 |
| No. of reflections | 2243 |
| No. of parameters | 173 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.33, −0.22 |