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. 2016 Sep 5;72(Pt 10):1366–1369. doi: 10.1107/S205698901601344X

Table 2. Experimental details.

Crystal data
Chemical formula C32H34N4O2
M r 506.63
Crystal system, space group Monoclinic, P21/c
Temperature (K) 100
a, b, c (Å) 5.1776 (3), 27.9346 (17), 8.7893 (6)
β (°) 96.203 (2)
V3) 1263.79 (14)
Z 2
Radiation type Mo Kα
μ (mm−1) 0.08
Crystal size (mm) 0.20 × 0.15 × 0.12
 
Data collection
Diffractometer Bruker SMART APEX CCD
Absorption correction Multi-scan (SADABS; Bruker, 2003)
T min, T max 0.783, 0.990
No. of measured, independent and observed [I > 2σ(I)] reflections 15125, 2243, 1469
R int 0.073
(sin θ/λ)max−1) 0.596
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.050, 0.127, 1.02
No. of reflections 2243
No. of parameters 173
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.33, −0.22

Computer programs: SMART and SAINT (Bruker, 2003), SIR97 (Altomare et al., 1999), DIAMOND (Brandenberg & Putz, 2006), SHELXL97 (Sheldrick, 2008) and PLATON (Spek, 2009).