| Crystal data |
| Chemical formula |
[Zn(C8H4NO2)2(C10H14N2O)2(H2O)2] |
|
M
r
|
750.13 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
7.4916 (3), 8.5915 (3), 15.0343 (6) |
| α, β, γ (°) |
86.363 (3), 75.894 (2), 74.390 (2) |
|
V (Å3) |
903.87 (6) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.74 |
| Crystal size (mm) |
0.45 × 0.30 × 0.24 |
| |
| Data collection |
| Diffractometer |
Bruker SMART BREEZE CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2012 ▸) |
|
T
min, T
max
|
0.74, 0.84 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
19149, 4366, 4029 |
|
R
int
|
0.020 |
| (sin θ/λ)max (Å−1) |
0.666 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.032, 0.084, 1.06 |
| No. of reflections |
4366 |
| No. of parameters |
242 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.56, −0.23 |
