Bruker APEXII CCD diffractometer | 5384 reflections with I > 2σ(I) |
φ and ω scans | Rint = 0.074 |
Absorption correction: multi-scan (SADABS; Sheldrick, 2003) | θmax = 28.3°, θmin = 2.9° |
Tmin = 0.635, Tmax = 0.746 | h = −8→9 |
36728 measured reflections | k = −19→21 |
9449 independent reflections | l = −43→42 |