Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C17H38ClN2 +·C32H12BF24 |
| M r | 1289.27 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 125 |
| a, b, c (Å) | 18.5025 (12), 17.8739 (12), 19.7857 (13) |
| β (°) | 116.428 (1) |
| V (Å3) | 5859.5 (7) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.18 |
| Crystal size (mm) | 0.39 × 0.38 × 0.08 |
| Data collection | |
| Diffractometer | Siemens/Bruker APEXII |
| Absorption correction | Multi-scan (SADABS; Bruker, 2008 ▸) |
| T min, T max | 0.660, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 40063, 10921, 8363 |
| R int | 0.033 |
| (sin θ/λ)max (Å−1) | 0.606 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.044, 0.113, 1.02 |
| No. of reflections | 10921 |
| No. of parameters | 830 |
| No. of restraints | 38 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.52, −0.45 |