Table 1. Nm ΔN-PilE data collection and refinement statistics.
| Data collection | Nm ΔN-PilE |
|---|---|
| Beamline | SSRL 7-1 |
| Wavelength (Å) | 0.9753 |
| Space group | P212121 |
| Cell a, b, c (Å) | 43. 5, 46.3, 48.4 |
| Cell α, β, γ (°) | 90.0, 90.0, 90.0 |
| Resolution (Å) | 1.44 |
| Completeness (%) | 98.7 (88.1)* |
| No. of observed reflections | 118934 |
| No. of unique reflections | 18088 |
| Rmeas (%) | 6 .0 (60.7) |
| R-factorobs | 5.5 (53.9) |
| I/σ(I) | 21.6 (2.8) |
| Wilson B value (Å2) | 18.7 |
| Mosaicity (°) | 0.5 |
| Refinement | |
| Resolution limits (Å) | 33.43-1.44 |
| Z | 4 |
| No. of reflections used | 18030 |
| Rcryst (%) | 18.7 |
| Rfree (%) | 21.0 |
| No. of non-hydrogen atoms: | |
| Protein | 1037 |
| Water | 156 |
| Avg B factor (Å2): | |
| Protein | 16.5 |
| Water oxygen | 24.8 |
| RMSD bond lengths (Å) | 0.004 |
| RMSD bond angles (°) | 0.679 |
| Ramachandron plot | |
| Favoured (%) | 94.2 |
| Allowed (%) | 5.8 |
| Outlier (%) | 0 |
| PDB ID | 5JW8 |
RMSD, root mean squared deviation
*Values in parenthesis represent the highest resolution shell.