Table 2. Data collection and refinement statistics.
| Agrobacterium radiobacter strain K84AgnB2 LeuRS+tRNALeu+Leu-AMS | |
|---|---|
| Data collection | |
| Space group | P21 |
| Cell dimensions | |
| a, b, c (Å) | 169.91, 50.32, 170.52 |
| α, β, γ (°) | 90.00, 93.48, 90.00 |
| Resolution (Å)* | 50-2.1 (2.10-2.20) |
| Rsym | 7.5 (65.2) |
| I/σI | 10.6 (2.0) |
| Completeness (%) | 99.5 (99.8) |
| Redundancy | 3.7 (3.7) |
| Refinement | |
| Resolution (Å) | 48.6-2.1 (2.15-2.10) |
| No. of reflections work/free | 160,330/8,487 |
| Rwork/Rfree | 0.194 (0.309)/0.237 (0.331) |
| No. of atoms | |
| Protein | [6,307]A, [6,141]B |
| tRNALeu | [1,702]C, [1,721]D |
| Ligand | 62 [2 × Leu-AMS] |
| Water/SO4−2 | 871/25 [5 × SO4−2] |
| Mn2+ | 2 |
| B-factors | |
| Protein | [52.3]A, [48.6]B |
| tRNALeu | [57.7]C, [54.9]D |
| Ligand | [27.8]E, [26.6]F |
| Water/SO4−2 | 44.4/86.2 |
| Mn2+ | 87.3 |
| RMS deviations | |
| Bond lengths (Å) | 0.016 |
| Bond angles (°) | 1.736 |
Values in brackets correspond to averages of the corresponding chain, indicated as superscript.
*Values in parentheses are for the highest-resolution shell.