Table 1. Data collection and refinement statistics.
| SeMet Nop9 (46–645) | Nop9 (46–645) | |
|---|---|---|
| Data collection | ||
| Space group | P21 | P21 |
| Cell dimensions | ||
| a, b, c (Å) | 67.58, 109.14, 115.04 | 67.50, 110.47, 114.85 |
| β (°) | 93.3 | 92.2 |
| Resolution (Å) | 50–2.65 (2.7–2.65)* | 50–2.1 (2.14–2.1) |
| Rsym | 0.114 (0.54) | 0.086 (0.43) |
| I/σI | 14.3 (2.75) | 12.5 (3.34) |
| Completeness (%) | 96.4 (72.0) | 97.5 (86.4) |
| Redundancy | 13.2 (6.8) | 7.0 (4.0) |
| Refinement | ||
| Resolution (Å) | 32.0–2.1 | |
| No. of reflections | 96,076 | |
| Rwork/Rfree | 18.5%/22.6% | |
| No. of atoms | 9,186 | |
| Protein | 8,809 | |
| Water/ion | 377 | |
| B-factors | ||
| Protein | 58.4 | |
| Water/ion | 53.7 | |
| R.m.s. deviations | ||
| Bond lengths (Å) | 0.009 | |
| Bond angles (°) | 1.11 | |
SeMet, selenomethionine.
*Values in parentheses are for the highest-resolution shell.