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. Author manuscript; available in PMC: 2017 Aug 1.
Published in final edited form as: Pharmacogenet Genomics. 2016 Aug;26(8):370–380. doi: 10.1097/FPC.0000000000000226

Table 1.

UPLC conditions for detection of phase I exemestane metabolites.

Time (min) % Aa % B % C curve
initial 70 20 10 initial
0.5 70 20 10 11
9 30 60 10 6
9.5 0 90 10 6
10 70 20 10 6
a

Mobile phase A, 0.1% formic acid; mobile phase B, 100% methanol; mobile phase C, 100% acetonitrile. Flow rate = 0.4 mL/min.