Table 3.
| |||
---|---|---|---|
Entry | substrate | product | Yield [%][a] |
1 | n/a | No fluorination | |
2 | Trace | ||
3 | Trace | ||
4 | Trace | ||
5 | Trace | ||
6 | n/a | No fluorination | |
7 | n/a | No fluorination | |
8 | Trace | ||
9 | 13 | ||
10 | 10 | ||
11 | 26[b] | ||
12 | n/a | No fluorination | |
13 | n/a | No fluorination | |
14 | n/a | No fluorination |
Yield determined by NMR through integration relative to a methyl acetate internal standard;
1.6:1 C2/C3 fluorination