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. Author manuscript; available in PMC: 2017 Jul 25.
Published in final edited form as: Angew Chem Int Ed Engl. 2016 Jun 20;55(31):8923–8927. doi: 10.1002/anie.201603149

Table 3.

Fluorination of Oxygenated Molecules

graphic file with name nihms805967u4.jpg
Entry substrate product Yield [%][a]
1 graphic file with name nihms805967t15.jpg n/a No fluorination
2 graphic file with name nihms805967t16.jpg graphic file with name nihms805967t17.jpg Trace
3 graphic file with name nihms805967t18.jpg graphic file with name nihms805967t19.jpg Trace
4 graphic file with name nihms805967t20.jpg graphic file with name nihms805967t21.jpg Trace
5 graphic file with name nihms805967t22.jpg graphic file with name nihms805967t23.jpg Trace
6 graphic file with name nihms805967t24.jpg n/a No fluorination
7 graphic file with name nihms805967t25.jpg n/a No fluorination
8 graphic file with name nihms805967t26.jpg graphic file with name nihms805967t27.jpg Trace
9 graphic file with name nihms805967t28.jpg graphic file with name nihms805967t29.jpg 13
10 graphic file with name nihms805967t30.jpg graphic file with name nihms805967t31.jpg 10
11 graphic file with name nihms805967t32.jpg graphic file with name nihms805967t33.jpg 26[b]
12 graphic file with name nihms805967t34.jpg n/a No fluorination
13 graphic file with name nihms805967t35.jpg n/a No fluorination
14 graphic file with name nihms805967t36.jpg n/a No fluorination
[a]

Yield determined by NMR through integration relative to a methyl acetate internal standard;

[b]

1.6:1 C2/C3 fluorination