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. 2016 Aug 5;(114):54236. doi: 10.3791/54236
Detector FID TOF-MS NCD
Injector  573 K 573 K 573 K
Split flow  30 ml/min 30 ml/min 10 ml/min
Carrier gas 2.1 ml/min 2.6 ml/min 2.1 ml/min
Initial oven temperature 233 K 233 K 233 K
Heating rate ramp I 4 K/min 4 K/min 4 K/min
Temperature hold, min 4 4 4
Temperature ramp 313 K 313 K 313 K
Heating rate ramp II 5 K/min 5 K/min 5 K/min
Final temperature 573 K 573 K 573 K
Modulation time 5 sec 5 sec 5 sec
Detector
Temperature 573 K 473 K 1,198 K
Range 10 n.a. 1
Acquisition rate 100 Hz 30 Hz 100 Hz