Table 1. Analyses conducted on ochre residue samples.
SEM-EDS | μ-RS | XRD | ||||
---|---|---|---|---|---|---|
Num | Sample* | Num of an | Sample* | Num of an | Sample* | Num of an |
1 | AT1A | 14 | AT1A, B | 5 | T1 | 1 |
2 | AT2A, B | 14 | AT2A, B | 7 | - | - |
3 | AT3 | 12 | AT3 | 5 | T3 | 1 |
4 | AT4 | 8 | AT4 | 6 | - | - |
5 | AT5 | 11 | AT5 | 4 | T5 | 1 |
6 | AT6B | 9 | AT6A | 3 | T6 | 1 |
7 | AT7 | 13 | AT7 | 12 | T7 | 1 |
8 | - | - | AT8 | 5 | T8 | 1 |
9 | AT9 | 15 | AT9 | 8 | T9 | 1 |
10 | - | - | AT10 | 8 | T10 | 1 |
11 | - | - | AT11 | 9 | - | - |
12 | AT12 | 6 | AT12 | 5 | T12 | 1 |
13 | AT13 | 9 | AT13 | 4 | - | - |
14 | - | - | AT14 | 7 | - | - |
15 | AT15 | 9 | AT15 | 7 | - | - |
16 | - | - | AT16 | 6 | - | - |
17 | - | - | AT17 | 9 | T17 | 1 |
18 | - | - | AT18 | 7 | T18 | 1 |
19 | - | - | AT19 | 7 | - | - |
20 | - | - | - | - | - | - |
21 | - | - | - | - | - | - |
22 | AT22 | 18 | AT22 | 2 | - | - |
23 | - | - | - | - | - | - |
Num: number; An: analyses; SEM-EDS: Scanning electron microscopy coupled with energy dispersive X-ray spectroscopy; μ-RS: micro-Raman spectroscopy; XRD: X-ray diffraction. The objects' identification number is the same as presented in Figs 4–11, Tables 2–5, S1 and S2 Figs, S1 Table, S1 Text.
* Samples AT1–AT19, AT22 refer to residues stuck on carbon adhesive tabs, and samples T1, T3, T5–T10, T12, T17, T18 refer to loose residues kept in sample tubes.