RIGAKU R-AXIS RAPID II diffractometer | 2087 independent reflections |
Radiation source: rotating anode X-ray | 1762 reflections with I > 2σ(I) |
Detector resolution: 10.0 pixels mm-1 | Rint = 0.036 |
ω–scan | θmax = 68.2°, θmin = 3.6° |
Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | h = −17→17 |
Tmin = 0.789, Tmax = 0.924 | k = −5→5 |
12627 measured reflections | l = −20→21 |