Table 2. Validation data for protein-bound BMAA.
Fortified Lamb’s Brain Samples |
|||
---|---|---|---|
3 μg/g | 9 μg/g | 30 μg/g | |
Intra-day RSD (%) (n = 6) | 6.5 | 2 | 4.6 |
Inter-day RSD (%) (n = 18) | 5 | 5.3 | 3.6 |
Average conc. (repeatability) (μg/g) | 2.87 | 8.87 | 30.90 |
Average conc. (reproducibility) (μg/g) | 2.91 | 9.05 | 30.28 |
Absolute recovery (%)* | 80 | 85 | 86 |
*Absolute recovery expressed as the extraction efficiency when spiked at 4 μg toxin per g brain.