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IR spectroscopic characterization of the bound HNO ligand in (PPDME)Fe(HNO)(1-MeIm), showing formation of the υNO 1384 cm−1 band (dashed line) upon hydride addition to the cationic precursor (υNO 1915 cm−1). The new 1384 cm−1 band slowly converts to the band at 1672 cm−1.
