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. Author manuscript; available in PMC: 2017 Nov 15.
Published in final edited form as: Dalton Trans. 2016 Nov 15;45(45):18259–18266. doi: 10.1039/c6dt03860c

Fig. 3.

Fig. 3

1H NMR spectra (in CDCl3) of the reaction of [(PPDME)Fe(NO)(1-MeIm)]OTf with [NBu4]BH4 to generate (PPDME)Fe(HNO)(1-MeIm). The bottom spectrum showing the splitting of the Fe-HNO peak at 13.64 ppm into a doublet was obtained using [(PPDME)Fe(15NO)(1-MeIm)]OTf in the reaction. The peak labeled * is due to the H2 decomposition product (see text and Fig. S2).