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11B{1H} NMR spectra of the product mixtures from (a) the reaction of [(OEP)Fe(NO)(5-MeIm)]OTf with excess [NBu4]BH4 (signal at −40 ppm), and (b) the reaction of [(OEP)Fe(NO)]OTf with excess [NBu4]BH4, and (c) the control and known reaction of [NBu4]BH4 with 1,2-dichloroethane to generate diborane.25
