Table 1. Data collection and refinement statistics.
| GltTKapo | GltTKsub | |
|---|---|---|
| Data collection | ||
| Space group | P3221 | |
| Cell dimensions | ||
| a, b, c (Å) | 116.01 116.01 308.5 | |
| α, β, γ (°) | 90.00, 90.00, 120.00 | |
| Resolution (Å) | 47.7–2.7(2.78–2.7)* | 48.4–2.8(2.87–2.8)* |
| Rmeas | 0.06 (0.74) | 0.07 (0.98) |
| CC1/2 | 99.6 (36.0) | 99.8 (22.1) |
| I/σI | 11(2.49) | 9.3(1.3) |
| Completeness (%) | 79(17.9) | 97.5 (96.0) |
| Redundancy | 3.4 | 3 |
| Refinement | ||
| Resolution (Å) | 2.7 | 2.8 |
| No. reflections | 52,820 | 60,568 |
| Rwork/Rfree (%) | 19.8/23.7 | 21.3/24.3 |
| No. atoms | ||
| Protein | 9,638 | 9,570 |
| PEG/detergent | 278/40 | 508/99 |
| Ligand/ion | – | 27/9 |
| Water | 60 | – |
| B-factors | ||
| Protein | 77.6 | 96.3 |
| PEG/detergent | 114/132 | 118.4/137.7 |
| Ligand/ion | – | 77.6/76.1 |
| Water | 69.9 | – |
| r.m.s. deviations | ||
| Bond lengths (Å) | 0.008 | 0.008 |
| Bond angles (°) | 1.123 | 1.131 |
*Values in parentheses are for the highest-resolution shell.