Table 1.
Data collection and refinement statistics.
|
NPAS-ARNT |
NPAS3-ARNT-DNA |
|
|---|---|---|
|
Data collection |
||
Space group |
P 1 |
P 43 |
Cell dimensions |
||
a, b, c (Å) |
69.9, 81.2, 138.1 |
64.8, 64.8, 249.1 |
α, β, γ (°) |
90.4, 95.1, 107.4 |
90.0, 90.0, 90.0 |
Resolution (Å) |
50.0–3.20 (3.26–3.20)* |
50.0–4.20 (4.27–4.20) |
Rmerge |
5.5 (76.4) |
6.0 (84.8) |
CC* (highest resolution shell) |
0.793 |
0.971 |
CC1/2 (highest resolution shell) |
0.459 |
0.893 |
|
I/σI |
14.0 (1.2) |
20.0 (1.1) |
Completeness (%) |
98.6 (98.3) |
94.6 (72.3) |
Redundancy |
2.1 (2.2) |
5.2 (3.9) |
|
Refinement |
||
Resolution (Å) |
37.7–3.20 (3.32–3.20) |
36.9–4.20 (5.28–4.20) |
No. reflections |
39,096 (802) |
5868 (2120) |
Rwork/ Rfree (%) |
19.2/24.9 (28.3/40.4) |
29.5/36.2 (27.1/34.8) |
No. atoms |
||
Protein/DNA |
13,303 |
5313 |
Water |
0 |
0 |
B-factors |
||
Protein/DNA |
49.6 |
66.9 |
Water |
- |
- |
R.m.s deviations |
||
Bond lengths (Å) |
0.016 |
0.004 |
Bond angles (°) |
1.46 |
0.77 |
One crystal was used for each structure.
*Highest resolution shell is shown in parenthesis.