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. Author manuscript; available in PMC: 2016 Nov 17.
Published in final edited form as: Tetrahedron. 2012 Apr 14;68(24):4635–4640. doi: 10.1016/j.tet.2012.04.025

Table 2. 13 C NMR data of compounds 1–6 in CDCl3.

No. 1a 2b 3b 4b 5b 6b
1 174.9 qC 175.7 qC 175.1 qC 175.0 qC 175.6 qC 166.8 qC
2 37.6 CH2 38.8 CH2 38.8 CH2 38.8 CH2 38.9 CH2 84.0 CH
3 72.4 CH 74.4 CH 74.6 CH 74.6 CH 74.5 CH 171.4 qC
4 93.3 qC 92.8 qC 92.3 qC 92.2 qC 92.7 qC 140.3 qC
5 120.1 CH 123.4 CH 124.0 CH 123.5 CH 124.0 CH 139.4 CH
6 148.6 qC 147.3 qC 147.3 qC 147.7 qC 147.0 qC 97.4 qC
7 44.9 CH2 37.5 CH2 41.4 CH2 35.1 CH2 44.7 CH2 43.6 CH2
8 30.8 CH 30.6 CH 32.6 CH 37.0 CH 30.9 CH 139.0 qC
9 36.5 CH2 37.1 CH2 36.8 CH2 33.1 CH2 36.8 CH2 132.9 CH
10 29.2CH2 29.2 CH2 28.8 CH2 29.2 CH2 29.3 CH2 69.6 CH
11 22.9 CH2 22.9 CH2 23.1 CH2 23.1 CH2 23.0 CH2 30.4 CH2
12 14.0 CH3 14.1 CH3 14.1 CH3 14.1 CH3 14.1 CH3 9.7 CH3
13 31.8 CH2 27.4 CH2 27.2 CH2 27.4 CH2 27.1 CH2 18.5 CH2
14 8.1 CH3 8.3 CH3 8.4 CH3 8.4 CH3 8.4 CH3 12.1 CH3
15 23.9 CH2 29.8 CH2 23.4 CH2 30.0 CH2 23.5 CH2 30.9 CH2
16 12.9 CH3 13.0 CH3 12.8 CH3 13.1 CH3 12.8 CH3 8.1 CH3
17 19.6 CH3 19.1 CH3 25.5 CH2 26.1 CH2 19.5 CH3 24.5 CH2
18 10.6 CH3 11.6 CH3 13.6 CH3
19 50.6 CH3
a

Recorded at 150 MHz.

b

Recorded at 125 MHz.