Table 2. 13 C NMR data of compounds 1–6 in CDCl3.
| No. | 1a | 2b | 3b | 4b | 5b | 6b |
|---|---|---|---|---|---|---|
| 1 | 174.9 qC | 175.7 qC | 175.1 qC | 175.0 qC | 175.6 qC | 166.8 qC |
| 2 | 37.6 CH2 | 38.8 CH2 | 38.8 CH2 | 38.8 CH2 | 38.9 CH2 | 84.0 CH |
| 3 | 72.4 CH | 74.4 CH | 74.6 CH | 74.6 CH | 74.5 CH | 171.4 qC |
| 4 | 93.3 qC | 92.8 qC | 92.3 qC | 92.2 qC | 92.7 qC | 140.3 qC |
| 5 | 120.1 CH | 123.4 CH | 124.0 CH | 123.5 CH | 124.0 CH | 139.4 CH |
| 6 | 148.6 qC | 147.3 qC | 147.3 qC | 147.7 qC | 147.0 qC | 97.4 qC |
| 7 | 44.9 CH2 | 37.5 CH2 | 41.4 CH2 | 35.1 CH2 | 44.7 CH2 | 43.6 CH2 |
| 8 | 30.8 CH | 30.6 CH | 32.6 CH | 37.0 CH | 30.9 CH | 139.0 qC |
| 9 | 36.5 CH2 | 37.1 CH2 | 36.8 CH2 | 33.1 CH2 | 36.8 CH2 | 132.9 CH |
| 10 | 29.2CH2 | 29.2 CH2 | 28.8 CH2 | 29.2 CH2 | 29.3 CH2 | 69.6 CH |
| 11 | 22.9 CH2 | 22.9 CH2 | 23.1 CH2 | 23.1 CH2 | 23.0 CH2 | 30.4 CH2 |
| 12 | 14.0 CH3 | 14.1 CH3 | 14.1 CH3 | 14.1 CH3 | 14.1 CH3 | 9.7 CH3 |
| 13 | 31.8 CH2 | 27.4 CH2 | 27.2 CH2 | 27.4 CH2 | 27.1 CH2 | 18.5 CH2 |
| 14 | 8.1 CH3 | 8.3 CH3 | 8.4 CH3 | 8.4 CH3 | 8.4 CH3 | 12.1 CH3 |
| 15 | 23.9 CH2 | 29.8 CH2 | 23.4 CH2 | 30.0 CH2 | 23.5 CH2 | 30.9 CH2 |
| 16 | 12.9 CH3 | 13.0 CH3 | 12.8 CH3 | 13.1 CH3 | 12.8 CH3 | 8.1 CH3 |
| 17 | 19.6 CH3 | 19.1 CH3 | 25.5 CH2 | 26.1 CH2 | 19.5 CH3 | 24.5 CH2 |
| 18 | 10.6 CH3 | 11.6 CH3 | 13.6 CH3 | |||
| 19 | 50.6 CH3 |
Recorded at 150 MHz.
Recorded at 125 MHz.