. 2016 Dec;90(6):689–702. doi: 10.1124/mol.116.105130

TABLE 2.

Analytical chiral column conditions and characterization of each enantiomer

	Analytical OD-RH Solvent Composition				ChiralPak OD-RH Retention Time		Optical Rotation Values
	ACN	H₂O	Flow Rate	Run Time	Peak 1	Peak 2	Peak 1	Peak 2
			ml/min	min	min	min	degrees	degrees
CIQ	75%	25%	0.5	20	16.81	19.32	+121 (c 0.10, dry DMSO)	−145 (c 0.10, dry DMSO)
BIQ	75%	25%	0.5	20	8.61	9.79	+104 (c 0.1, dry CHCl₃)	−128 (c 0.1, dry CHCl₃)
IIQ	65%	35%	0.5	30	17.33	19.89	+106 (c 0.1, dry CHCl₃)	−93 (c 0.1, dry CHCl₃)
FIQ	60%	40%	0.5	30	13.47	15.53	+89.4 (c 1.0, dry CHCl₃)	−102 (c 1.0, dry CHCl₃)