Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C35H30N4O3 |
| M r | 554.63 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 293 |
| a, b, c (Å) | 10.1194 (4), 10.8066 (4), 14.9948 (6) |
| α, β, γ (°) | 110.57 (2), 97.10 (2), 106.17 (2) |
| V (Å3) | 1429.1 (4) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.08 |
| Crystal size (mm) | 0.35 × 0.30 × 0.25 |
| Data collection | |
| Diffractometer | Bruker Kappa APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2004 ▸) |
| T min, T max | 0.719, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 42242, 8042, 4733 |
| R int | 0.034 |
| (sin θ/λ)max (Å−1) | 0.717 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.046, 0.140, 1.03 |
| No. of reflections | 8042 |
| No. of parameters | 383 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.23, −0.20 |