Skip to main content
. 2016 Aug 12;72(Pt 9):1285–1289. doi: 10.1107/S2056989016012494
O3—H3 0.95 (4) O1—H1 0.81 (4)
O3—B2 1.371 (3) O1—B1 1.368 (3)
O4—H4 0.89 (4) O2—H2 0.90 (3)
O4—B2 1.363 (3) O2—B1 1.364 (3)
C11—C12 1.381 (4) C1—C2 1.379 (4)
C11—C20 1.438 (3) C1—C10 1.436 (3)
C11—B2 1.570 (4) C1—B1 1.572 (4)
C12—H12 0.97 (3) C2—H2A 0.9500
C12—C13 1.422 (5) C2—C3 1.410 (4)
C13—H13 0.88 (4) C3—H3A 0.9500
C13—C14 1.353 (5) C3—C4 1.363 (4)
C14—H14 1.07 (4) C4—H4A 0.9500
C14—C15 1.403 (4) C4—C5 1.413 (4)
C15—C16 1.422 (4) C5—C6 1.426 (4)
C15—C20 1.435 (3) C5—C10 1.424 (3)
C16—H16 1.00 (4) C6—H6 0.9500
C16—C17 1.355 (5) C6—C7 1.353 (4)
C17—H17 1.02 (4) C7—H7 0.9500
C17—C18 1.400 (4) C7—C8 1.405 (4)
C18—H18 1.03 (4) C8—H8 0.9500
C18—C19 1.373 (3) C8—C9 1.373 (4)
C19—H19 0.9500 C9—H9 0.9500
C19—C20 1.415 (3) C9—C10 1.417 (3)
B2—O3—H3 119 (2) B1—O1—H1 116 (3)
B2—O4—H4 113 (2) B1—O2—H2 113 (2)
C12—C11—C20 117.9 (2) C2—C1—C10 118.1 (2)
C12—C11—B2 119.0 (2) C2—C1—B1 117.8 (2)
C20—C11—B2 123.1 (2) C10—C1—B1 124.1 (2)
C11—C12—H12 119.2 C1—C2—H2A 118.9
C11—C12—C13 121.6 (3) C1—C2—C3 122.3 (3)
C13—C12—H12 119.2 C3—C2—H2A 118.9
C12—C13—H13 119.7 C2—C3—H3A 119.9
C14—C13—C12 120.5 (3) C4—C3—C2 120.1 (2)
C14—C13—H13 119.7 C4—C3—H3A 119.9
C13—C14—H14 119.5 C3—C4—H4A 119.9
C13—C14—C15 121.0 (3) C3—C4—C5 120.3 (3)
C15—C14—H14 119.5 C5—C4—H4A 119.9
C14—C15—C16 122.1 (3) C4—C5—C6 120.9 (2)
C14—C15—C20 119.1 (3) C4—C5—C10 119.8 (2)
C16—C15—C20 118.8 (3) C10—C5—C6 119.3 (2)
C15—C16—H16 119.0 C5—C6—H6 119.5
C17—C16—C15 122.0 (3) C7—C6—C5 121.1 (2)
C17—C16—H16 119.0 C7—C6—H6 119.5
C16—C17—H17 120.2 C6—C7—H7 119.9
C16—C17—C18 119.6 (3) C6—C7—C8 120.1 (3)
C18—C17—H17 120.2 C8—C7—H7 119.9
C17—C18—H18 119.7 C7—C8—H8 119.7
C19—C18—C17 120.5 (3) C9—C8—C7 120.6 (3)
C19—C18—H18 119.7 C9—C8—H8 119.7
C18—C19—H19 119.0 C8—C9—H9 119.4
C18—C19—C20 122.0 (2) C8—C9—C10 121.2 (2)
C20—C19—H19 119.0 C10—C9—H9 119.4
C15—C20—C11 119.8 (2) C5—C10—C1 119.3 (2)
C19—C20—C11 123.0 (2) C9—C10—C1 122.9 (2)
C19—C20—C15 117.1 (2) C9—C10—C5 117.8 (2)
O3—B2—C11 122.1 (2) O1—B1—C1 121.8 (2)
O4—B2—O3 116.9 (2) O2—B1—O1 117.1 (2)
O4—B2—C11 121.1 (2) O2—B1—C1 121.0 (2)
C11—C12—C13—C14 −0.4 (4) C1—C2—C3—C4 0.3 (4)
C12—C11—C20—C15 −0.3 (3) C2—C1—C10—C5 0.2 (3)
C12—C11—C20—C19 178.6 (2) C2—C1—C10—C9 −178.3 (2)
C12—C11—B2—O3 −38.2 (3) C2—C1—B1—O1 37.5 (3)
C12—C11—B2—O4 140.1 (2) C2—C1—B1—O2 −140.3 (2)
C12—C13—C14—C15 0.0 (4) C2—C3—C4—C5 0.0 (4)
C13—C14—C15—C16 −178.8 (3) C3—C4—C5—C6 179.0 (2)
C13—C14—C15—C20 0.2 (4) C3—C4—C5—C10 −0.2 (3)
C14—C15—C16—C17 179.2 (3) C4—C5—C6—C7 −178.4 (2)
C14—C15—C20—C11 0.0 (3) C4—C5—C10—C1 0.1 (3)
C14—C15—C20—C19 −179.1 (2) C4—C5—C10—C9 178.7 (2)
C15—C16—C17—C18 −0.3 (4) C5—C6—C7—C8 −0.5 (4)
C16—C15—C20—C11 179.0 (2) C6—C5—C10—C1 −179.2 (2)
C16—C15—C20—C19 0.0 (3) C6—C5—C10—C9 −0.6 (3)
C16—C17—C18—C19 0.2 (4) C6—C7—C8—C9 −0.1 (4)
C17—C18—C19—C20 0.0 (4) C7—C8—C9—C10 0.4 (4)
C18—C19—C20—C11 −179.1 (2) C8—C9—C10—C1 178.5 (2)
C18—C19—C20—C15 −0.1 (3) C8—C9—C10—C5 0.0 (3)
C20—C11—C12—C13 0.5 (3) C10—C1—C2—C3 −0.4 (3)
C20—C11—B2—O3 140.8 (2) C10—C1—B1—O1 −142.0 (2)
C20—C11—B2—O4 −41.0 (3) C10—C1—B1—O2 40.3 (3)
C20—C15—C16—C17 0.2 (4) C10—C5—C6—C7 0.9 (3)
B2—C11—C12—C13 179.6 (2) B1—C1—C2—C3 −179.9 (2)
B2—C11—C20—C15 −179.3 (2) B1—C1—C10—C5 179.7 (2)
B2—C11—C20—C19 −0.3 (3) B1—C1—C10—C9 1.2 (3)