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. 2016 Aug 16;72(Pt 9):1310–1314. doi: 10.1107/S2056989016012937
C1—C16 1.411 (3) C12—C13 1.420 (3)
C1—C2 1.426 (3) C13—C14 1.349 (3)
C1—C12 1.434 (3) C13—H13 0.9300
C2—C3 1.373 (3) C14—C15 1.405 (3)
C2—C17 1.492 (3) C14—H14 0.9300
C3—C10 1.423 (3) C15—C16 1.358 (3)
C3—S1 1.7492 (19) C15—H15 0.9300
C4—C5 1.384 (3) C16—H16 0.9300
C4—C9 1.397 (3) C17—C18 1.375 (3)
C4—S1 1.746 (2) C17—C22 1.376 (3)
C5—C6 1.372 (3) C18—C19 1.377 (3)
C5—H5 0.9300 C18—H18 0.9300
C6—C7 1.388 (3) C19—C20 1.370 (3)
C6—H6 0.9300 C19—H19 0.9300
C7—C8 1.373 (3) C20—C21 1.366 (3)
C7—H7 0.9300 C20—C23 1.508 (3)
C8—C9 1.393 (3) C21—C22 1.382 (3)
C8—H8 0.9300 C21—H21 0.9300
C9—C10 1.449 (3) C22—H22 0.9300
C10—C11 1.369 (3) C23—H23A 0.9600
C11—C12 1.400 (3) C23—H23B 0.9600
C11—H11 0.9300 C23—H23C 0.9600
C16—C1—C2 122.80 (18) C14—C13—H13 119.2
C16—C1—C12 117.81 (17) C12—C13—H13 119.2
C2—C1—C12 119.39 (17) C13—C14—C15 120.2 (2)
C3—C2—C1 117.87 (17) C13—C14—H14 119.9
C3—C2—C17 120.13 (17) C15—C14—H14 119.9
C1—C2—C17 121.99 (17) C16—C15—C14 120.2 (2)
C2—C3—C10 123.09 (17) C16—C15—H15 119.9
C2—C3—S1 125.07 (15) C14—C15—H15 119.9
C10—C3—S1 111.84 (14) C15—C16—C1 121.9 (2)
C5—C4—C9 121.40 (19) C15—C16—H16 119.1
C5—C4—S1 125.91 (16) C1—C16—H16 119.1
C9—C4—S1 112.68 (15) C18—C17—C22 117.15 (19)
C6—C5—C4 118.5 (2) C18—C17—C2 122.18 (17)
C6—C5—H5 120.8 C22—C17—C2 120.65 (17)
C4—C5—H5 120.8 C17—C18—C19 121.4 (2)
C5—C6—C7 121.0 (2) C17—C18—H18 119.3
C5—C6—H6 119.5 C19—C18—H18 119.3
C7—C6—H6 119.5 C20—C19—C18 121.4 (2)
C8—C7—C6 120.6 (2) C20—C19—H19 119.3
C8—C7—H7 119.7 C18—C19—H19 119.3
C6—C7—H7 119.7 C21—C20—C19 117.3 (2)
C7—C8—C9 119.6 (2) C21—C20—C23 121.5 (2)
C7—C8—H8 120.2 C19—C20—C23 121.2 (2)
C9—C8—H8 120.2 C20—C21—C22 121.7 (2)
C8—C9—C4 118.95 (19) C20—C21—H21 119.1
C8—C9—C10 128.82 (18) C22—C21—H21 119.1
C4—C9—C10 112.23 (17) C17—C22—C21 121.0 (2)
C11—C10—C3 118.90 (18) C17—C22—H22 119.5
C11—C10—C9 129.40 (18) C21—C22—H22 119.5
C3—C10—C9 111.69 (17) C20—C23—H23A 109.5
C10—C11—C12 120.75 (18) C20—C23—H23B 109.5
C10—C11—H11 119.6 H23A—C23—H23B 109.5
C12—C11—H11 119.6 C20—C23—H23C 109.5
C11—C12—C13 121.63 (19) H23A—C23—H23C 109.5
C11—C12—C1 120.00 (17) H23B—C23—H23C 109.5
C13—C12—C1 118.37 (18) C4—S1—C3 91.52 (9)
C14—C13—C12 121.6 (2)
C16—C1—C2—C3 −179.76 (17) C10—C11—C12—C1 −0.5 (3)
C12—C1—C2—C3 −0.2 (3) C16—C1—C12—C11 −179.63 (17)
C16—C1—C2—C17 −0.5 (3) C2—C1—C12—C11 0.8 (3)
C12—C1—C2—C17 179.12 (16) C16—C1—C12—C13 0.1 (3)
C1—C2—C3—C10 −0.6 (3) C2—C1—C12—C13 −179.48 (18)
C17—C2—C3—C10 −179.96 (16) C11—C12—C13—C14 179.1 (2)
C1—C2—C3—S1 179.27 (13) C1—C12—C13—C14 −0.6 (3)
C17—C2—C3—S1 −0.1 (3) C12—C13—C14—C15 0.6 (4)
C9—C4—C5—C6 −1.3 (3) C13—C14—C15—C16 −0.1 (3)
S1—C4—C5—C6 179.61 (17) C14—C15—C16—C1 −0.4 (3)
C4—C5—C6—C7 −0.3 (3) C2—C1—C16—C15 179.98 (18)
C5—C6—C7—C8 1.3 (4) C12—C1—C16—C15 0.4 (3)
C6—C7—C8—C9 −0.7 (3) C3—C2—C17—C18 −108.5 (2)
C7—C8—C9—C4 −0.9 (3) C1—C2—C17—C18 72.2 (3)
C7—C8—C9—C10 178.1 (2) C3—C2—C17—C22 70.1 (3)
C5—C4—C9—C8 1.9 (3) C1—C2—C17—C22 −109.1 (2)
S1—C4—C9—C8 −178.87 (15) C22—C17—C18—C19 −0.7 (3)
C5—C4—C9—C10 −177.24 (18) C2—C17—C18—C19 177.9 (2)
S1—C4—C9—C10 2.0 (2) C17—C18—C19—C20 0.3 (4)
C2—C3—C10—C11 0.9 (3) C18—C19—C20—C21 0.4 (4)
S1—C3—C10—C11 −179.04 (15) C18—C19—C20—C23 −179.5 (2)
C2—C3—C10—C9 179.87 (17) C19—C20—C21—C22 −0.6 (4)
S1—C3—C10—C9 0.0 (2) C23—C20—C21—C22 179.3 (2)
C8—C9—C10—C11 −1.4 (3) C18—C17—C22—C21 0.5 (3)
C4—C9—C10—C11 177.64 (19) C2—C17—C22—C21 −178.2 (2)
C8—C9—C10—C3 179.71 (19) C20—C21—C22—C17 0.2 (4)
C4—C9—C10—C3 −1.2 (2) C5—C4—S1—C3 177.47 (19)
C3—C10—C11—C12 −0.3 (3) C9—C4—S1—C3 −1.69 (15)
C9—C10—C11—C12 −179.05 (18) C2—C3—S1—C4 −178.95 (17)
C10—C11—C12—C13 179.71 (18) C10—C3—S1—C4 0.96 (14)