| Bruker Kappa APEXII CCD diffractometer | 3171 independent reflections |
| Radiation source: fine-focus sealed tube | 2540 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.036 |
| ω & φ scans | θmax = 25.0°, θmin = 2.5° |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −14→14 |
| Tmin = 0.946, Tmax = 0.955 | k = −39→39 |
| 43542 measured reflections | l = −10→9 |