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. 2016 Aug 16;72(Pt 9):1310–1314. doi: 10.1107/S2056989016012937
Bruker Kappa APEXII CCD diffractometer 3171 independent reflections
Radiation source: fine-focus sealed tube 2540 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.036
ω & φ scans θmax = 25.0°, θmin = 2.5°
Absorption correction: multi-scan (SADABS; Bruker, 2008) h = −14→14
Tmin = 0.946, Tmax = 0.955 k = −39→39
43542 measured reflections l = −10→9