TABLE 1.
Data collection and refinement statistics
| Data collection | |
| Beamline | SSRF 17U |
| Space group | P 21 21 21 |
| Cell dimensions | |
| a, b, c (Å) | 42.40, 119.36, 141.59 |
| α, β, γ (degrees) | 90, 90, 90 |
| Wavelength (Å) | 0.97923 |
| Resolution (Å) | 91.26–2.70 (2.83–2.70)a |
| Total no. of observations | 127,579 (15,093) |
| Total no. of unique observations | 18,674 (2271) |
| Rmerge (%) | 0.095 (1.065) |
| I/σI | 12.3 (1.7) |
| Completeness (%) | 90.9 (84.6) |
| Multiplicity | 6.3 (6.6) |
| Refinement | |
| Resolution (Å) | 91.26–2.70 (2.77–2.70) |
| No. of reflections | 17,694 (1197) |
| No. of residues | 732 |
| No. of atoms | 5704 |
| Rwork/Rfree | 0.223/0.284 |
| B-factors (Å2) | 62.3 |
| RMSD | |
| Bond lengths (Å) | 0.0088 |
| Bond angles (degrees) | 1.3057 |
| Ramachandran plot | 97.77/0 |
a Values in parentheses are for the highest resolution shell.