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. 2016 Nov 25;10:71. doi: 10.1186/s13065-016-0218-4

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© The Author(s) 2016

Open AccessThis article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The Creative Commons Public Domain Dedication waiver (http://creativecommons.org/publicdomain/zero/1.0/) applies to the data made available in this article, unless otherwise stated.

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Fig. 2 — Synthetic routes of complexes. (i) 4 h reflux in 10:1 acetonitrile:water mixture (ii) 0.16 h reflux in water (iii) 0.16 h reflux in water (iv). 8 h reflux in 7:2:1 acetonitrile:methanol:water mixture