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. 2016 Oct 28;14(11):200. doi: 10.3390/md14110200

Table 1.

Comparison of 1H NMR data of isolated compounds 2 (in MeOH-d4) and 3 (in DMSO-d6) with literature data recorded in the identical solvents [14,15].

Position Alternariol (2) Alternariol-9-methylether (3)
Isolated a Literature a Isolated a Literature b
H-2 6.55, d (2.6) 6.55, d (2.5) 6.72, d (2.6) 6.72, d (2.3)
H-4 6.64, d (2.6) 6.65, d (2.5) 6.64, d (2.6) 6.64, d (2.4)
H-8 6.31, d (2.1) 6.32, d (2.0) 6.61, d (2.2) 6.61, d (2.3)
H-10 7.20, d (2.1) 7.20, d (2.0) 7.23, d (2.2) 7.21, d (2.3)
5-CH3 2.70, s 2.71, s 2.73, s 2.73, s
O-CH3 - - 3.90, s 3.90, s
3-OH - - 10.38, brs 10.36, brs
7-OH - - 11.82, brs 11.81, brs

a recorded at 500 MHz; b recorded at 400 MHz.