Table 1.
Position | Alternariol (2) | Alternariol-9-methylether (3) | ||
---|---|---|---|---|
Isolated a | Literature a | Isolated a | Literature b | |
H-2 | 6.55, d (2.6) | 6.55, d (2.5) | 6.72, d (2.6) | 6.72, d (2.3) |
H-4 | 6.64, d (2.6) | 6.65, d (2.5) | 6.64, d (2.6) | 6.64, d (2.4) |
H-8 | 6.31, d (2.1) | 6.32, d (2.0) | 6.61, d (2.2) | 6.61, d (2.3) |
H-10 | 7.20, d (2.1) | 7.20, d (2.0) | 7.23, d (2.2) | 7.21, d (2.3) |
5-CH3 | 2.70, s | 2.71, s | 2.73, s | 2.73, s |
O-CH3 | - | - | 3.90, s | 3.90, s |
3-OH | - | - | 10.38, brs | 10.36, brs |
7-OH | - | - | 11.82, brs | 11.81, brs |
a recorded at 500 MHz; b recorded at 400 MHz.