Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [Ir(C11H8N)2(C18H14N)] |
| M r | 744.87 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 173 |
| a, b, c (Å) | 19.8293 (3), 8.6464 (1), 18.1551 (3) |
| β (°) | 106.715 (1) |
| V (Å3) | 2981.21 (8) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 4.51 |
| Crystal size (mm) | 0.30 × 0.25 × 0.17 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2013 ▸) |
| T min, T max | 0.521, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 27408, 6855, 6080 |
| R int | 0.033 |
| (sin θ/λ)max (Å−1) | 0.651 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.026, 0.062, 1.02 |
| No. of reflections | 6855 |
| No. of parameters | 397 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.77, −0.71 |