| Crystal data |
| Chemical formula |
[Cu(C5H5NO2S2)(C18H15P)2]·CHCl3
|
|
M
r
|
887.71 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
10.7271 (2), 13.5412 (2), 15.9361 (3) |
| α, β, γ (°) |
67.747 (2), 87.126 (2), 72.826 (2) |
|
V (Å3) |
2041.92 (7) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.95 |
| Crystal size (mm) |
0.44 × 0.24 × 0.19 |
| |
| Data collection |
| Diffractometer |
Rigaku SuperNova, Dual Mo at zero, AtlasS2 |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku Oxford Diffraction, 2015 ▸) |
|
T
min, T
max
|
0.928, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
78295, 11363, 10195 |
|
R
int
|
0.029 |
| (sin θ/λ)max (Å−1) |
0.708 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.045, 0.117, 1.03 |
| No. of reflections |
11363 |
| No. of parameters |
478 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.97, −1.93 |
