Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C24H16N2O4 |
| M r | 396.39 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 173 |
| a, b, c (Å) | 6.1500 (5), 4.7475 (3), 31.002 (2) |
| β (°) | 90.461 (3) |
| V (Å3) | 905.14 (11) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.10 |
| Crystal size (mm) | 0.50 × 0.06 × 0.02 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker 2013 ▸) |
| T min, T max | 0.661, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 4593, 2016, 1444 |
| R int | 0.034 |
| (sin θ/λ)max (Å−1) | 0.650 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.048, 0.119, 1.04 |
| No. of reflections | 2016 |
| No. of parameters | 136 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.25, −0.22 |