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. 2016 Nov 15;72(Pt 12):1809–1811. doi: 10.1107/S2056989016017710

Table 2. Experimental details.

Crystal data
Chemical formula C24H16N2O4
M r 396.39
Crystal system, space group Monoclinic, P21/n
Temperature (K) 173
a, b, c (Å) 6.1500 (5), 4.7475 (3), 31.002 (2)
β (°) 90.461 (3)
V3) 905.14 (11)
Z 2
Radiation type Mo Kα
μ (mm−1) 0.10
Crystal size (mm) 0.50 × 0.06 × 0.02
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Bruker 2013)
T min, T max 0.661, 0.746
No. of measured, independent and observed [I > 2σ(I)] reflections 4593, 2016, 1444
R int 0.034
(sin θ/λ)max−1) 0.650
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.048, 0.119, 1.04
No. of reflections 2016
No. of parameters 136
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.25, −0.22

Computer programs: APEX2 and SAINT (Bruker, 2013), SHELXS97 and SHELXTL (Sheldrick 2008), SHELXL2014 (Sheldrick, 2015) and DIAMOND (Brandenburg, 2010).