Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C5H4ClNOSe |
| M r | 208.50 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 3.9601 (8), 7.5102 (15), 22.350 (5) |
| β (°) | 94.32 (3) |
| V (Å3) | 662.8 (2) |
| Z | 4 |
| Radiation type | Synchrotron, λ = 0.96990 Å |
| μ (mm−1) | 13.68 |
| Crystal size (mm) | 0.05 × 0.03 × 0.03 |
| Data collection | |
| Diffractometer | Rayonix SX-165 CCD |
| Absorption correction | Multi-scan (SCALA; Evans, 2006 ▸) |
| T min, T max | 0.550, 0.660 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 5526, 1310, 1121 |
| R int | 0.083 |
| (sin θ/λ)max (Å−1) | 0.636 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.074, 0.175, 1.01 |
| No. of reflections | 1310 |
| No. of parameters | 83 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.26, −1.58 |