Table 2. Diffraction statistics for ten X-ray data sets collected from the crystallization screening plate.
R sym is defined as ∑(I − 〈I〉)2/∑I 2.
| Crystal | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 |
|---|---|---|---|---|---|---|---|---|---|---|
| Unit cell a = b, c (Å) | 79.27, 37.63 | 79.44, 37.78 | 79.43, 37.69 | 79.29, 37.70 | 79.26, 37.71 | 79.25, 37.83 | 79.26, 37.74 | 79.46, 37.82 | 79.26, 37.72 | 79.27, 37.72 |
| Resolution (Å) | 50–1.26 (1.28–1.26) | 50–1.31 (1.33–1.31) | 50–1.31 (1.33–1.31) | 50–1.31 (1.33–1.31) | 50–1.50 (1.52–1.50) | 50–1.21 (1.23–1.21) | 50–1.37 (1.39–1.37) | 50–1.34 (1.36–1.34) | 50–1.25 (1.27–1.25) | 50–1.23 (1.25–1.23) |
| Unique reflections | 29163 | 25138 | 25055 | 23524 | 15096 | 32640 | 20285 | 21719 | 28058 | 29547 |
| Completeness (%) | 91 | 88 | 87 | 82 | 78 | 90 | 81 | 81 | 85 | 85 |
| Redundancy | 1.1 | 1.2 | 1.2 | 1.2 | 1.3 | 1.1 | 1.2 | 1.2 | 1.2 | 1.2 |
| 〈I/σ(I)〉 | 29 (2) | 34 (3) | 28 (2) | 26 (2) | 20 (2) | 34 (3) | 32 (2) | 30 (2) | 37 (3) | 34 (3) |
| R sym | 0.105 (0.99) | 0.091 (0.95) | 0.065 (0.69) | 0.081 (0.84) | 0.100 (0.95) | 0.063 (0.66) | 0.073 (0.72) | 0.076 (0.68) | 0.086 (0.83) | 0.064 (0.64) |