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. Author manuscript; available in PMC: 2017 Nov 15.
Published in final edited form as: Biochemistry. 2016 Nov 2;55(45):6205–6208. doi: 10.1021/acs.biochem.6b00982

Scheme 1. Synthesis of the phosphoramidite for 2′-fluoroarabino-5-formyldeoxycytidinea.

Scheme 1

aKey: a) TBSCl b) Pd2(dba)3, PPh3, Bu3SnH, CO c) 1,3-Propanediol, triethyl orthoformate, TiCl4 d) p-Methoxybenzoyl chloride e) HF•pyridine f) DMTCl g) Phosphitylation.