. Author manuscript; available in PMC: 2017 Nov 15.

Published in final edited form as: Bioorg Med Chem Lett. 2016 Oct 6;26(22):5513–5516. doi: 10.1016/j.bmcl.2016.10.010

Table 2.

Analytical data of cyclic Dyn A analogues

no	molecular formula	MS^a		HPLC^b (t_R,min)	Purity (%)	aLogPs^c
no	molecular formula	calculated	observed	HPLC^b (t_R,min)	Purity (%)	aLogPs^c
2	C₃₁H₅₅N₉O₇	666.4	666.4	15.0	95	−2.25
3	C₃₁H₅₇N₉O₇	668.4	668.5	11.6	95	−2.17
5	C₄₄H₇₄N₁₄O₉	943.6	943.7	14.1	98	−2.24
6	C₄₁H₇₇N₁₅O₉	924.6	924.5	11.9	98	−2.35
7	C₃₅H₆₅N₁₃O₈	796.5	796.5	11.7	98	−2.74

(M + H)⁺, ESI method (Finnigan, Thermoelectron, LCQ classic).

Performed on a Hewlett Packard 1100 (C-18, Microsorb-MV™, 4.6 mm × 250 mm, 5 μm) using gradient system (10–100% of acetonitrile containing 0.1% TFA within 45 min, 1 mL/min).

http://www.vcclab.org/lab/alogps.