Table 1.
ICP-MS tuning parameters | |
---|---|
Oxide ratio (156/140) | 0.775% |
Doubly charged (70/140) | 1.485% |
Plasma condition | |
RF power | 1200 W |
RF matching | 1.76 V |
Sample depth | 8 mm |
Torch horizontal | 0.8 mm |
Torch vertical | 0 mm |
Carrier gas | 1.02 L/min |
Nebulizer pump | 0.1 r/s |
S/C temperature | 2 °C |
Ion lenses | |
Extract 1 | −101.2 V |
Extract 2 | −5 V |
Einzel 1, 3 | −100 V |
Einzel 2 | 11 V |
Omega bias | −40 V |
Omega (+) | 2.4 V |
Omega (−) | −2 V |
QP focus | 2 V |
Plate bias | −4.2 V |
Q-pole parameters | |
AMU gain | 130 |
AMU offset | 125 |
Axis gain | 0.9998 |
QP bias | −8 V |
Detector parameters | |
Discriminator | 8 mV |
Analog HV | 1740 V |
Pulse HV | 1200 V |
S/C: spray chamber; AMU: atomic mass unit; QP: Q-pole; HV: high voltage.