Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C34H26F2O6 |
| M r | 568.55 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 200 |
| a, b, c (Å) | 16.2618 (7), 11.6708 (5), 14.7359 (7) |
| β (°) | 96.945 (2) |
| V (Å3) | 2776.2 (2) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.10 |
| Crystal size (mm) | 0.63 × 0.29 × 0.15 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2009 ▸) |
| T min, T max | 0.894, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 38582, 6911, 5302 |
| R int | 0.020 |
| (sin θ/λ)max (Å−1) | 0.668 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.040, 0.106, 1.01 |
| No. of reflections | 6911 |
| No. of parameters | 379 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.32, −0.39 |