| Bruker SMART APEXII CCD diffractometer | 6655 reflections with I > 2σ(I) |
| Radiation source: fine focus sealed tube | Rint = 0.021 |
| phi and ω scans | θmax = 36.2°, θmin = 2.2° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2014) | h = −14→13 |
| Tmin = 0.667, Tmax = 0.747 | k = −24→24 |
| 43306 measured reflections | l = −19→12 |
| 7519 independent reflections |
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