Refinement on F2	Secondary atom site location: difference Fourier map
Least-squares matrix: full	Hydrogen site location: mixed
R[F2 > 2σ(F2)] = 0.025	H atoms treated by a mixture of independent and constrained refinement
wR(F2) = 0.068	w = 1/[σ2(Fo2) + (0.0357P)2 + 0.4526P] where P = (Fo2 + 2Fc2)/3
S = 1.02	(Δ/σ)max = 0.003
7519 reflections	Δρmax = 0.60 e Å−3
221 parameters	Δρmin = −0.44 e Å−3
6 restraints	Extinction correction: SHELXL2014 (Sheldrick, 2015), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
Primary atom site location: structure-invariant direct methods	Extinction coefficient: 0.0025 (3)