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. 2017 Jan 1;73(Pt 1):38–40. doi: 10.1107/S2056989016019733

Table 2. Experimental details.

Crystal data
Chemical formula C23H29N3O
M r 363.49
Crystal system, space group Monoclinic, P21/c
Temperature (K) 293
a, b, c (Å) 11.565 (2), 8.0504 (16), 20.665 (4)
β (°) 97.68 (3)
V3) 1906.7 (7)
Z 4
Radiation type Mo Kα
μ (mm−1) 0.08
Crystal size (mm) 0.18 × 0.14 × 0.11
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Bruker, 2005)
T min, T max 0.894, 0.943
No. of measured, independent and observed [I > 2σ(I)] reflections 15990, 3900, 2582
R int 0.077
(sin θ/λ)max−1) 0.625
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.064, 0.150, 1.06
No. of reflections 3900
No. of parameters 286
No. of restraints 2
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.33, −0.25

Computer programs: APEX2 and SAINT (Bruker, 2005), SHELXS97 (Sheldrick, 2008), SHELXL2014 (Sheldrick, 2015), ORTEP-3 for Windows (Farrugia, 2012), Mercury (Macrae et al., 2008) and PLATON (Spek, 2009).